Version2.1 2021-01-06T15:08:22Z 10.1021/jm300687e Gaussian16 RevisionB.01 PWARBURT 21-Nov-2020 #N HF/6-31G(d) OPT=(MaxStep=1) FREQ IOp(6/10=2,6/11=2,6/12=2) DUDE CC(C)[C@H](C(=O)OCC(=O)c1c[nH]c2c1cccc2)NS(=O)(=O)c3ccc4c(c3)OCCO4 C02618876 RHF 6-31G(d) (6D,7F) CC(C)[C@H](C(=O)OCC(=O)c1c[nH]c2c1cccc2)NS(=O)(=O)c3ccc4c(c3)OCCO4 C01[X(C23H24N2O7S1)] 165 C1 547 CC([C@H](C(=O)OCC(=O)c1c[nH]c2c1cccc2)NS(=O)(=O)c1ccc2c(c1)OCCO2)C CC([C@H](C(=O)OCC(=O)c1c[nH]c2c1cccc2)NS(=O)(=O)c1ccc2c(c1)OCCO2)C CC(C)[C@@H](N[S](=O)(=O)c1ccc2OCCOc2c1)C(=O)OCC(=O)c3c[nH]c4ccccc34 InChIKey=GZBQTZOWVZWLSQ-JOCHJYFZSA-N InChI=1S/C23H24N2O7S/c1-14(2)22(25-33(28,29)15-7-8-20-21(11-15)31-10-9-30-20)23(27)32-13-19(26)17-12-24-18-6-4-3-5-16(17)18/h3-8,11-12,14,22,24-25H,9-10,13H2,1-2H3/t22-/m1/s1 InChI=1/C23H24N2O7S/c1-14(2)22(25-33(28,29)15-7-8-20-21(11-15)31-10-9-30-20)23(27)32-13-19(26)17-12-24-18-6-4-3-5-16(17)18/h3-8,11-12,14,22,24-25H,9-10,13H2,1-2H3/t22-/m1/s1 CC(C)[C@H](C(=O)OCC(=O)c1c[nH]c2c1cccc2)NS(=O)(=O)c3ccc4c(c3)OCCO4 C01[X(C23H24N2O7S1)] 165 C01 547 CC([C@H](C(=O)OCC(=O)c1c[nH]c2c1cccc2)NS(=O)(=O)c1ccc2c(c1)OCCO2)C CC([C@H](C(=O)OCC(=O)[C]1[CH]N[C]2[C]1[CH][CH][CH][CH]2)N[S@]([O])(=O)[C]1[CH][CH][C]2[C]([CH]1)OCCO2)C CC(C)[C@@H](N[S]([O])(=O)[C]1[CH][CH][C]2OCCO[C]2[CH]1)C(=O)OCC(=O)[C]3[CH]N[C]4[CH][CH][CH][CH][C]34 InChIKey=NRVXVIZOYAMSME-JOCHJYFZSA-N InChI=1S/C23H24N2O7S/c1-14(2)22(25-33(28,29)15-7-8-20-21(11-15)31-10-9-30-20)23(27)32-13-19(26)17-12-24-18-6-4-3-5-16(17)18/h3-8,11-12,14,22,24H,9-10,13H2,1-2H3,(H,25,28,29)/t22-/m1/s1 InChI=1/C23H24N2O7S/c1-14(2)22(25-33(28,29)15-7-8-20-21(11-15)31-10-9-30-20)23(27)32-13-19(26)17-12-24-18-6-4-3-5-16(17)18/h3-8,11-12,14,22,24H,9-10,13H2,1-2H3,(H,25,28,29)/t22-/m1/s1/f/h25H 3528.4329147969 -1915.3297056 1-A 22961.8309 124 423 547 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1385.35 1395.72 1410.45 1416.60 1457.64 1466.00 1474.55 1486.17 1492.09 1510.93 1511.36 1546.96 1560.37 1574.65 1601.03 1608.18 1611.19 1681.73 1691.30 1713.61 1728.09 1737.60 1748.44 1770.80 1775.09 1782.42 1786.96 1793.37 1812.13 1825.60 1846.39 1863.71 1870.32 1930.66 1956.21 1973.09 1978.81 1997.29 2003.94 2022.01 2025.71 2038.54 2042.84 2084.20 2092.46 2092.92 2128.64 2145.53 2192.47 2196.86 2211.07 2244.60 2252.06 2262.77 2272.86 2282.57 2293.38 2338.25 2342.35 2346.16 2358.92 2366.71 2373.49 2380.48 2384.48 2387.61 2395.72 2419.67 2467.18 2559.33 2570.27 2596.45 2621.78 2856.23 2881.72 4604.38 4610.32 4624.37 4642.60 4657.65 4685.66 4692.52 4716.39 4723.00 4747.45 4752.84 4757.27 4770.10 4772.01 4829.86 4847.46 4869.24 4885.45 4911.49 4923.66 4926.77 4955.44 5420.18 5630.50 0.485017 0.513398 0.514342 0.419543 -1914.844689 -1914.816308 -1914.815363 -1914.910162 3.179574D-04 MUNgauss RevisionA2.0 retrievium 06-Jan-2021 DUDE CC(C)[C@H](C(=O)OCC(=O)c1c[nH]c2c1cccc2)NS(=O)(=O)c3ccc4c(c3)OCCO4 C02618876 RHF 6-31G(d) (6D,10F) C1 472.130423 |X|Y|Z| 132.221239 61.548401 41.124143 69.428580 26 6 7 8 16 20 2 3 1 |36.858105| |12.444872|36.858105| |7.563606|12.423056|36.858105| |7.540707|12.326231|7.460233|36.858105| |7.042479|8.829424|6.660715|17.626919|0.500000| |4.912036|7.525136|6.495845|12.513338|0.248495|36.858105| |4.167170|6.025600|5.244607|7.975922|0.164936|16.012621|73.516695| |4.202588|5.809720|6.027811|8.067800|0.219350|14.476436|15.260287|73.516695| |3.245718|4.215351|4.525828|5.180976|0.139132|8.188182|12.762706|24.085184|36.858105| |2.870846|3.519186|3.994513|4.039662|0.115681|5.284760|8.214625|14.219403|12.515623|36.858105| |3.038264|3.650245|4.337561|4.053773|0.120955|4.876484|7.258657|12.893465|8.035630|15.949949|73.516695| |2.356101|2.792935|3.090345|3.133025|0.088599|3.930165|6.579888|9.105764|7.490387|12.974879|14.494175|36.858105| |2.155029|2.543347|2.722256|2.868015|0.079340|3.620512|6.404805|7.793415|6.371067|7.507330|9.399968|13.987502|36.858105| |1.878999|2.164992|2.316734|2.387437|0.066428|2.881510|5.112830|5.982436|4.407372|5.215509|7.438022|8.553713|14.072336|53.358707| |1.744950|1.995426|2.107531|2.193082|0.060633|2.618794|4.726344|5.274539|3.769107|4.178207|6.141621|5.993318|9.123430|26.105563|0.500000| |1.843104|2.098395|2.287691|2.278506|0.064363|2.680400|4.635326|5.644612|3.981557|5.138638|7.889702|8.348393|8.541356|18.802357|0.249886|36.858105| |2.081932|2.392748|2.667709|2.603869|0.074488|3.083116|5.170805|6.800248|4.849932|7.314616|11.394652|13.135243|8.464867|11.582549|0.165448|13.648677|36.858105| |2.032912|2.289757|2.593977|2.437708|0.070771|2.775506|4.577871|6.051211|3.974076|5.769842|10.775025|7.255859|5.239373|7.289368|0.118587|7.903649|13.614869|36.858105| |1.780048|1.969478|2.201928|2.073375|0.059918|2.314092|3.876756|4.859975|3.110973|4.093680|7.513668|5.008902|4.174002|6.329479|0.109459|6.959984|7.986871|13.853300|36.858105| |1.624226|1.796069|1.973641|1.898556|0.054279|2.130170|3.638790|4.383834|2.843546|3.561745|6.188480|4.545871|4.189169|7.022175|0.126283|8.067749|6.869254|7.865591|13.571204|36.858105| |1.644328|1.838401|1.998728|1.966578|0.055698|2.249722|3.897847|4.620328|3.096378|3.817441|6.258055|5.258167|5.302758|10.331383|0.184961|13.679078|7.786740|6.732523|7.870508|13.858332|36.858105| |6.409369|7.769544|4.990523|13.055908|0.254778|7.816302|12.041644|9.670735|4.082307|3.245396|5.648517|2.670056|2.537026|2.927751|0.055891|2.029634|2.255695|2.104100|1.827485|1.702132|1.773307|53.358707| |4.390987|4.783001|3.651593|7.122394|0.190712|5.804763|9.307166|8.350052|3.765056|3.068114|5.267786|2.598157|2.510949|2.918561|0.056126|2.010074|2.206254|2.046322|1.790057|1.681721|1.761103|15.701119|388.023441| |3.660074|3.893433|3.049179|5.045608|0.129011|4.480652|7.970088|6.515918|3.147418|2.597923|4.410567|2.278856|2.258132|2.667959|0.052091|1.822812|1.960009|1.813985|1.610559|1.533159|1.613120|10.592045|94.713620|73.516695| |3.758546|4.294785|3.560654|6.551268|0.189027|6.436878|9.947093|10.114058|4.610199|3.674423|6.145557|3.081959|2.980998|3.392303|0.064706|2.312181|2.553896|2.326328|2.008093|1.885665|1.992998|10.257499|94.449424|13.616182|73.516695| |4.436217|4.228671|3.335561|5.526233|0.171862|4.254057|6.614570|6.756950|3.081439|2.694035|4.817238|2.301649|2.183695|2.596984|0.049894|1.831115|2.017532|1.921583|1.698370|1.583484|1.631114|9.657349|76.783338|12.955685|13.106635|36.858105| |4.336778|3.837592|3.024410|4.483150|0.131648|3.482829|5.621688|5.504674|2.580067|2.291308|4.119572|1.990904|1.899660|2.292649|0.044352|1.623841|1.773461|1.704364|1.525236|1.427619|1.463709|7.865674|49.622943|11.104078|8.777983|13.699517|36.858105| |3.785541|3.247332|2.687871|3.599378|0.108461|2.891208|4.666758|4.748460|2.267205|2.074796|3.782505|1.822264|1.730156|2.115029|0.040957|1.514561|1.651789|1.608587|1.452339|1.356920|1.379401|5.712252|33.792915|7.727293|6.819834|7.982946|13.840005|36.858105| |3.446423|3.015321|2.596296|3.373863|0.106094|2.774123|4.407014|4.728477|2.267926|2.122352|3.915784|1.866217|1.756108|2.155351|0.041587|1.557098|1.706076|1.675859|1.514340|1.407616|1.422243|5.014278|29.985750|6.557008|6.600701|6.918439|7.944731|13.710899|36.858105| |3.498666|3.196973|2.787417|3.759041|0.124041|3.120919|4.841775|5.454552|2.586722|2.430455|4.500130|2.114824|1.973170|2.402281|0.046051|1.736928|1.919906|1.880931|1.683264|1.556228|1.574242|5.399156|33.768569|6.880721|7.948395|7.979400|6.852144|7.910838|13.718106|36.858105| |3.918220|3.756162|3.169145|4.809733|0.163188|3.913947|5.943366|6.713284|3.088819|2.804718|5.108360|2.395224|2.239489|2.675704|0.051100|1.909663|2.121111|2.041179|1.801219|1.666942|1.704719|7.112735|49.730107|8.967686|11.757946|13.784056|7.887290|6.859404|7.937565|13.765322|36.858105| |3.001983|2.799544|2.554560|3.226149|0.106518|2.801789|4.356111|5.090537|2.471722|2.400587|4.500454|2.113002|1.956644|2.406953|0.046043|1.761470|1.950490|1.935276|1.741569|1.603162|1.608133|4.414766|26.679159|5.569408|6.750167|5.266081|4.605877|5.210098|7.957360|14.048469|8.083410|73.516695| |2.746706|2.500222|2.320832|2.750371|0.088565|2.399273|3.781362|4.350480|2.143505|2.111543|3.992236|1.880714|1.741605|2.170088|0.041651|1.602225|1.765980|1.776449|1.619207|1.490100|1.481103|3.740119|21.551078|4.674712|5.328523|4.057758|3.885291|4.677094|7.071480|8.198852|5.313737|24.088455|36.858105| |2.568207|2.308688|2.107913|2.506923|0.078222|2.182745|3.508070|3.864421|1.920170|1.864473|3.473823|1.677596|1.575745|1.972030|0.038156|1.444986|1.573634|1.571946|1.443682|1.342494|1.341158|3.531698|20.477281|4.620148|4.885547|3.893164|4.038383|5.292486|8.171801|7.062409|4.676556|14.196333|12.587444|36.858105| |2.940877|2.567646|2.279785|2.771446|0.085798|2.343846|3.769230|4.052465|1.984215|1.891646|3.509527|1.686162|1.587542|1.972361|0.038172|1.435613|1.565196|1.552991|1.418580|1.320172|1.325114|4.010339|23.092449|5.235025|5.252232|4.643889|5.270629|8.098786|14.121790|7.978235|5.230440|12.099049|7.966134|13.513266|73.516695| |17.553505|8.820100|6.913803|5.487847|0.142005|4.069669|6.427379|6.358844|2.888239|2.606217|4.914393|2.176989|1.997834|2.397967|0.045608|1.736884|1.950932|1.920214|1.697069|1.550818|1.562883|6.615267|25.274918|5.532938|5.531618|3.584289|3.618565|3.281453|3.002087|2.985167|3.230408|4.666736|2.466615|2.334251|4.715149|0.500000| |17.605220|8.747760|5.485437|6.928627|0.177405|4.534509|7.086517|6.740759|2.990866|2.620187|4.834603|2.190364|2.036698|2.427883|0.046369|1.736352|1.936995|1.878831|1.658335|1.527719|1.554297|9.875269|35.062407|7.465018|6.982594|5.130071|5.346886|4.476087|3.836056|3.756565|4.226027|5.518688|2.826653|2.713042|5.691228|0.301378|0.500000| |17.527892|8.784714|6.898170|6.766278|0.206958|4.559034|6.675371|7.430332|3.210424|2.931886|5.665411|2.391863|2.156857|2.569025|0.048459|1.872292|2.133835|2.111216|1.845113|1.668304|1.674900|7.540472|29.872198|6.064087|6.627574|4.569025|4.375522|3.990066|3.799624|3.926634|4.289971|6.047536|3.126468|2.847896|5.768980|0.301756|0.301240|0.500000| |8.891728|17.514103|8.908869|8.932545|0.174991|6.817791|11.277420|8.930899|3.919340|3.216305|5.750853|2.627793|2.450221|2.852164|0.054153|2.008432|2.252605|2.134751|1.854057|1.711548|1.764725|9.970418|31.926139|6.946724|7.024482|3.798430|3.556697|2.990224|2.721287|2.827666|3.292559|4.408489|2.233718|2.103229|4.163835|0.214551|0.211147|0.173422|0.500000| |6.713465|8.741676|17.554412|6.830978|0.197851|5.953641|8.193967|11.149525|4.616488|4.332378|8.927637|3.268318|2.796377|3.244702|0.059677|2.394970|2.850276|2.827175|2.372617|2.090056|2.092242|6.218340|25.331583|5.177493|6.369560|3.387776|3.018998|2.735175|2.717781|2.979309|3.358542|4.945940|2.524051|2.240617|4.254535|0.165304|0.138439|0.199937|0.173383|0.500000| |5.483529|8.704612|17.572951|6.650129|0.159290|7.172688|10.761996|12.112415|5.360621|4.579049|8.548293|3.488490|3.066087|3.494543|0.064491|2.512328|2.943329|2.806545|2.354683|2.116498|2.164980|6.264070|24.676087|5.240476|6.221269|3.045896|2.735821|2.422688|2.346301|2.535100|2.902205|4.175625|2.125127|1.935581|3.680509|0.142303|0.122297|0.139486|0.215329|0.302136|0.500000| |7.075378|8.834216|17.562606|5.462500|0.139031|4.812917|7.474065|8.015497|3.666281|3.358874|6.487231|2.711798|2.416220|2.859956|0.053520|2.090769|2.407125|2.375730|2.053975|1.846882|1.856000|5.635700|22.239858|4.808691|5.329014|2.938799|2.760075|2.504616|2.408854|2.527048|2.790097|4.143361|2.165013|1.989069|3.830947|0.213255|0.142806|0.176266|0.211263|0.301303|0.302814|0.500000| |2.955947|3.712039|3.754681|4.706827|0.126859|7.099513|12.092941|16.654208|17.614334|8.800633|10.749956|6.927175|6.840778|6.293664|0.112151|3.960355|4.556014|3.650480|2.937620|2.761377|3.074751|5.449725|28.025683|5.935627|9.062431|3.137425|2.598690|2.269173|2.268590|2.601093|3.141752|4.413955|2.130806|1.920424|3.515956|0.072921|0.077857|0.081050|0.097733|0.105440|0.118202|0.086797|0.500000| |3.146640|4.152195|4.552970|4.761104|0.121196|7.463493|13.596115|16.508690|17.599468|8.905858|11.356633|6.587860|6.076808|5.869898|0.104281|3.832024|4.497116|3.696335|2.960484|2.747384|3.012162|5.225484|24.292622|5.268828|7.032023|2.786885|2.397184|2.108822|2.081143|2.321946|2.728595|3.920568|1.943609|1.765633|3.263464|0.079482|0.080339|0.084343|0.112124|0.122325|0.159325|0.104556|0.302089|0.500000| |2.197277|2.617721|2.733371|2.998921|0.081369|3.884347|7.152391|8.044997|6.685969|6.434094|8.187398|8.630022|17.792340|12.328210|0.215188|5.887651|5.762904|4.074589|3.381042|3.411901|4.187661|3.674979|19.124753|4.346069|5.720459|2.276204|1.974420|1.778098|1.787051|2.001656|2.298324|3.483573|1.733770|1.581868|2.853267|0.056338|0.058227|0.060363|0.071020|0.076504|0.085802|0.067094|0.223377|0.183510|0.500000| |2.208491|2.481429|2.867552|2.620992|0.077137|2.940677|4.740475|6.516599|4.106518|6.093307|13.079215|6.454521|4.551562|5.911291|0.099062|5.628014|8.869442|17.768294|8.908813|5.603616|4.882511|3.025053|15.209771|3.330696|4.300820|2.030820|1.798142|1.702018|1.781499|2.006862|2.171773|3.682334|1.904697|1.669479|2.933086|0.057875|0.056088|0.064443|0.063322|0.088968|0.085416|0.072734|0.101501|0.104480|0.102840|0.500000| |1.723638|1.881929|2.110130|1.958488|0.056875|2.143643|3.574989|4.451700|2.762557|3.535168|6.725541|4.033467|3.408726|5.014541|0.089615|4.997326|5.663402|8.972058|17.718362|8.887427|5.633115|2.354560|12.022078|2.707212|3.334928|1.625923|1.470461|1.411514|1.477483|1.635314|1.730183|3.026293|1.599621|1.424377|2.478767|0.045907|0.044542|0.049915|0.049081|0.063515|0.061923|0.055254|0.072154|0.073186|0.079507|0.214796|0.500000| |1.494960|1.636270|1.788140|1.717597|0.049059|1.902268|3.262893|3.852093|2.450350|2.968725|5.214294|3.618931|3.423893|5.628019|0.106481|5.697754|4.950237|5.628069|8.876330|17.716263|8.980196|2.115373|10.942278|2.511930|3.038992|1.459717|1.326093|1.267470|1.315344|1.445321|1.535224|2.653542|1.398488|1.265892|2.207374|0.039848|0.039199|0.042648|0.043465|0.052415|0.052863|0.046899|0.066433|0.066187|0.080435|0.123770|0.215669|0.500000| |1.525133|1.696827|1.824328|1.812652|0.051042|2.063707|3.619706|4.155736|2.758978|3.247760|5.298897|4.294400|4.625053|9.128910|0.188154|8.823844|5.567281|4.878194|5.599412|8.895570|17.711232|2.254605|11.760150|2.722963|3.308899|1.529930|1.380473|1.302056|1.338237|1.472964|1.590859|2.669046|1.386526|1.264997|2.222546|0.040373|0.040303|0.042956|0.045592|0.052568|0.054721|0.047307|0.077358|0.075385|0.107076|0.106317|0.123753|0.214789|0.500000| |5.510080|6.891263|4.622982|9.206591|0.180379|7.267519|13.265068|8.751467|3.921281|3.072466|5.242333|2.578460|2.497695|2.888679|0.055576|1.981804|2.175737|2.013179|1.758674|1.652761|1.733193|25.829898|61.957047|13.848682|11.119521|5.462383|4.830726|3.629071|3.165726|3.327066|4.183084|4.958399|2.411567|2.311179|4.632504|0.124764|0.171754|0.127956|0.211720|0.113133|0.123647|0.109596|0.107911|0.106666|0.074853|0.058485|0.046118|0.041999|0.045237|0.500000| |4.312463|3.838759|2.969542|4.342285|0.119810|3.411364|5.684382|5.245881|2.486647|2.182838|3.886935|1.908681|1.838208|2.221061|0.043167|1.564218|1.697383|1.623826|1.457498|1.371352|1.411167|8.088224|47.315861|12.283587|8.055157|8.891551|17.755116|8.935146|5.646707|4.944212|5.628522|6.501847|3.201729|3.356971|7.556621|0.101955|0.153587|0.114369|0.102959|0.080139|0.075154|0.076128|0.069598|0.065327|0.053441|0.047352|0.038976|0.035437|0.037110|0.146721|0.500000| |3.458023|2.932528|2.457042|3.125342|0.091778|2.557994|4.201755|4.198494|2.035421|1.873321|3.412844|1.661587|1.584552|1.951723|0.037949|1.399650|1.517592|1.482731|1.348488|1.264161|1.282857|4.916110|27.809611|6.709037|5.702120|5.649508|8.895000|17.743538|8.978203|5.654314|4.947512|7.505302|4.067287|4.848300|13.264930|0.086187|0.113788|0.099498|0.076513|0.068783|0.061701|0.064816|0.056439|0.053240|0.045202|0.043466|0.036524|0.032947|0.033757|0.089906|0.213335|0.500000| |3.649169|3.690731|3.220540|4.891334|0.170766|4.225697|6.295816|7.596298|3.494842|3.190925|5.789639|2.701472|2.507231|2.966928|0.056273|2.115435|2.368437|2.263544|1.976857|1.823210|1.870735|6.765834|47.143643|8.331160|13.662385|8.884198|5.616679|4.948733|5.655905|8.958265|17.765000|13.160438|4.841213|4.056410|7.510008|0.084216|0.104953|0.110874|0.089414|0.096377|0.083502|0.077514|0.100045|0.083323|0.071256|0.066919|0.052406|0.046331|0.048236|0.111941|0.123739|0.107498|0.500000| |2.425719|2.253182|2.131945|2.471484|0.078838|2.213674|3.512369|4.072057|2.043628|2.045026|3.869297|1.845194|1.709344|2.148718|0.041287|1.596084|1.752987|1.774688|1.630059|1.501378|1.485595|3.326370|19.137203|4.200141|4.852705|3.418287|3.231958|3.732910|5.127726|5.940344|4.373082|16.892268|17.635461|8.835281|10.155753|0.061207|0.068506|0.075903|0.056311|0.064548|0.054873|0.055397|0.056627|0.051441|0.046993|0.052727|0.044914|0.039281|0.038664|0.060346|0.076110|0.092660|0.117445|0.500000| |2.975989|2.649438|2.483389|2.846804|0.092414|2.448033|3.826819|4.450439|2.171239|2.151513|4.127141|1.898636|1.741452|2.166763|0.041423|1.609365|1.787461|1.813693|1.649046|1.505864|1.487999|3.788062|20.988207|4.515151|5.140520|3.895647|3.775218|4.511205|6.432366|7.030625|4.920170|16.545617|17.546439|8.881583|12.756659|0.074568|0.083873|0.096597|0.065006|0.075898|0.062310|0.064795|0.059074|0.054880|0.047929|0.054530|0.045473|0.039238|0.038548|0.067601|0.087405|0.110687|0.124749|0.299823|0.500000| |2.347794|2.154754|1.965741|2.369205|0.073136|2.098658|3.405877|3.712770|1.866553|1.807450|3.331591|1.642113|1.556066|1.953470|0.037961|1.424828|1.540064|1.529263|1.409351|1.319593|1.324154|3.380201|20.120668|4.621301|4.850677|3.755717|3.849666|4.865868|6.960283|6.384520|4.481552|12.794747|8.884347|17.558926|16.552167|0.059316|0.069118|0.071023|0.055089|0.057630|0.050724|0.051357|0.052439|0.047662|0.043552|0.044773|0.038504|0.034609|0.034830|0.062005|0.089906|0.124268|0.109959|0.213276|0.173864|0.500000| 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